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1 article(s) from Grirrane, Abdessamad

Isolation and X-ray characterization of palladium–N complexes in the guanylation of aromatic amines. Mechanistic implications

Abdessamad Grirrane,
Hermenegildo Garcia and
Eleuterio Álvarez

Beilstein J. Org. Chem. 2013, 9, 1455–1462, doi:10.3762/bjoc.9.165

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Scheme 1: Isolation of trans-dichlorobis(4-iodoanilino-ĸN)palladium(II) and trans-dichlorobis[1,3-diisopropyl...

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Scheme 2: Isolation of trans-dichlorobis[1,3-diisopropyl-2-(aryl)guanidino-ĸN(aryl)]palladium(II) complexes (...

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Figure 1: (Top) ORTEP view of the centrosymmetric molecule 4a. (Bottom) Crystal packing detail of 4a viewed a...

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Figure 2: (Left) ORTEP representation of 4b. (Right) Crystal packing detail of 4b viewed along the a-axis sho...

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Figure 3: (Left) ORTEP representation of 4c. (Right) Crystal-packing detail of 4c viewed along the a-axis sho...

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Scheme 3: Guanylation reactions of anilines 1a–c by N,N’-diisopropylcarbodiimide (2) catalyzed by Pd(II) salt....

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Figure 4: (Left) ORTEP representation of 5a. (Right) Crystal packing details of 5a viewed along the a-axis sh...

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Scheme 4: Possible mechanisms for the C–N coupling catalyzed by PdCl₂(NCMe)₂ in homogeneous phase.

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Published 22 Jul 2013

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